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Supercritical - Supercritical fluids laboratory scale extractor/precipitator (from 1.8 to 9.7 mL) equipped with membrane pump (P max 60 MPa) temperature control (SPE-ED, SFE, Applied Separation, USA) - High pressure optical cell (74 mL, P max 100MPa) withy two windows (diameter 18 mm) and temperature control (SITEC Switzerland); - 2 Syringe pumps, volume 260 mL, P Max 400 MPa(260D, Teledyne ISCO); - High pressure reactor/precipitator (150 mL); - HPLC pumps for co-solvent delivery (Waters, USA) Spectrometry Micro FT-IR - MFT 2000 Jasco ATR FT-IR UV-Visible - V-570 Jasco Elemental Analysis CHNS-O - FLASH EA 1112 Series Thermoquest Water content Karl-Fischer automatic volumetric titrator - Titromatic 15 Crison |
Thermal Analysis Differential Scanning Calorimeter - DSC 821/700 Mettler Toledo Thermo-gravimetric Analysis - TC15 TA, MT5 Balance Mettler Toledo Hot-Stage Microscope - Linkam HFS 91, Nikon Optiphot2- POL Diffractometry Bench-scale Powder X-ray diffractometer - Miniflex Rigaku Powder density Gas Pycnometer - Multivolume Pycnometer 1305 Micromeritics Powder dimension Laser light diffractometer - Mastersizer X Malvern High performance liquid chromatography Agilent 1100 -MS API 150EX Applied Biosystems Shimadzu LC 10AT VP - RID 10A & SPD M10A VP |
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